Improved Synthesis of tert-Butanesulfinamide Suitable for Large-Scale Production
Weix DJ, Ellman JA. Improved Synthesis of tert-Butanesulfinamide Suitable for Large-Scale Production. Organic Letters 2003, 5: 1317-1320. PMID: 12688748, DOI: 10.1021/ol034254b.Peer-Reviewed Original ResearchCatalytic asymmetric oxidationHomogeneous reaction conditionsChiral ligandsAsymmetric oxidationImproved synthesisReaction conditionsDi-tertButyl disulfidePrevious synthesesSolvent acetoneLarge-scale productionSingle stepSynthesisKey stepM concentrationLigandsOxidationAcetoneDisulfideReactionStepMaterials
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