RAPID HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY/TANDEM MASS SPECTROMETRY APCI METHOD FOR DETERMINATION OF NITROGEN CONTAINING COMPOUNDS IN PLASMA*
Nassar A, Varshney N, Getek T. RAPID HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY/TANDEM MASS SPECTROMETRY APCI METHOD FOR DETERMINATION OF NITROGEN CONTAINING COMPOUNDS IN PLASMA*. Analytical Letters 2001, 34: 2047-2062. DOI: 10.1081/al-100106838.Peer-Reviewed Original ResearchLimit of quantitationAtmospheric pressure chemical ionizationLC-APCI-MS/MSRat plasma samplesInternal standardRetention time precisionCalibration standard curvesHigh-performance liquid chromatography-mass spectrometryLiquid chromatography-mass spectrometryNitrogen-containing compoundsChemical ionizationGas chromatography/mass spectrometryDerivatization stepAPCI methodChromatography-mass spectrometryPlasma matrixContaining compoundsSpiked levelsLC-MS/MS analysisPerchloric acidRat plasmaAverage linear responseAnalysis timeSample preparationValidation parameters
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